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The present investigation was initiated to evaluate the wear resistance of filled and unfilled resins which may be suitable for fissure sealing. Two commercial unfilled resins (Adaptic Glaze and Delton), three degrees of diluted composite (Adaptic diluted with Adaptic Bonding Agent) and undiluted composite (Adaptic) were studied. Abrasion was caused by 400-grit silicon carbide paper in a mechanical surface grinder. Ten specimens of each of the material samples were tested. The unfilled resins were abraded three to six times more readily than the composite samples. Undiluted composite was the most resistant, whereas samples of increasing degrees of dilution were abraded to increasing extents. However, even the most diluted composite, although very fluid, was at least three times more resistant than the unfilled samples. The results of this study indicate that adding inorganic filler particles to a resin, even in small amounts, greatly enhances the wear resistance of such materials.
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PMID:Abrasive wear of filled and unfilled resins in vitro. 28 61

Two experimental methods were used to produce wear striations in one direction on unworn teeth. These include: (1) sliding 22 American Indian (Juntunen site, Michigan; Late Woodland) newly erupted incisors, by hand, across a flat grass surface covered with fine loose sand; and (2) using a unidirectional motor driven mechanical wear machine to draw 56 modern human dental extractions across a flat glass surface covered with silicon carbide powder of different grit sizes. A scanning electron microscope examination of individual wear striation morphology indicates that these wear striations begin with broad pits and have extending grooves that become narrower; characteristics that indicate the motion of wear. Patterns of wear striations on the worn dentitions of American Indians (Juntunen site) and the paleocene primate Phenacolemur pagei show similar characteristics and correspond to the buccal phase of mastication when the mandible is drawn upward, forward and slightly medially into centric occlusion. The data provided by this study can be used to test competing hypotheses concerning the direction of mandibular movement during mastication and food preparation.
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PMID:Wear striation direction on primate teeth: a scanning electron microscope examination. 44 53

This study evaluated the effect of dentin surface treatment with polyacrylic acid on the shear bond strength of Fuji Lining LC light-cured glass ionomer lining cement (GIC). A total of 40 human, noncarious extracted permanent molars stored in distilled water were used. A flat buccal dentin surface was ground wet on 600-grit silicon carbide paper. The teeth were then randomly distributed into four groups of 10 teeth each: Group 1: dentin rinsed with distilled water, dried with oil-free compressed air, placement of cylindrical GIC samples and sheared at 15 minutes post-curing. Group 2: same as group 1, but sheared 7 days post-curing. Group 3: dentin treated with GC Conditioner for 10 seconds, rinsed with distilled water, dried with oil-free compressed air, placement of the GIC and sheared 15 minutes post-curing. Group 4: same as group 3, but sheared 7 days post-curing. The GIC was mixed in a 1:1 powder-liquid ratio. The samples were stored in distilled water until sheared with an Instron. The results revealed that dentin surface treatment with the polyacrylic acid significantly increased the shear bond strength to dentin when tested at 7 days post-curing.
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PMID:Dentin surface treatment and shear bond strength of a light-cured glass ionomer. 129 59

The purpose of this study was to evaluate the effect of a fluoridated etching gel on the shear bond strength of a composite resin to enamel. A total of 75 extracted human permanent molars were used. A flat enamel surface was obtained with 600-grit silicon carbide paper and cleaned with a rubber cup and a water slurry of fine flour of pumice. The teeth were randomly distributed into 5 groups of 15 teeth each and etched as follows: group 1: 37% non-fluoridated phosphoric acid gel (Coe) for 60 seconds (control); group 2: 60% phosphoric acid gel with 0.5% NaF (Orthoprep) for 5 seconds; group 3: Orthoprep for 15 seconds; group 4: Orthoprep for 30 seconds; group 5: Orthoprep for 60 seconds. After etching, rinsing and drying, an unfilled resin (Coe Bond) was thinly applied with a brush and cured for 30 seconds. A nylon ring was placed over the area and filled with a light-cured composite resin (Occlusin). The teeth were thermocyled (100x), mounted in plastic cups and plaster, and sheared with a knife-edged blade in an Instron machine running at a crosshead speed of 1 mm/min. The results in MPa were as follows: group 1: 14.49 +/- 4.43; group 2: 10.81 +/- 3.70; group 3: 13.51 +/- 3.21; group 4: 14.79 +/- 3.76; group 5: 15.47 +/- 4.07. An analysis of variance showed that the results in groups 1, 4 and 5 were not significantly different but that the bond strengths in groups 2 and 3 were significantly lower. Fracture within the enamel occurred in 8 specimens in group 1, 5 in group 2, 6 in group 3, 8 in group 4, and 13 in group 5. In the fluoridated etchant groups the number of specimens showing enamel fracture increased as the application time of the etchant increased.
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PMID:Effect of a fluoridated etchant on the shear bond strength of a composite resin to enamel. 152 28

Adhesive bond strength studies for the tray adhesive of an addition vinyl polysiloxane (President) impression material were conducted with an acrylic resin, chromium-plated brass, and plastic trays. Tensile and shear stress studies were performed on the Instron Universal testing machine. Acrylic resin specimens roughened with 80-grit silicon carbide paper exhibited appreciably higher bond strengths compared with different types of tray material and methods of surface preparation.
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PMID:Properties of the tray adhesive of an addition polymerizing silicone to impression tray materials. 180 22

The aim of the present study was to evaluate the tensile bond strength of four dentinal bonding agents (DBAs) to the dentin surface. Tensile bond test procedure was made using a universal testing machine. Human extracted third molars were mounted with self-curing acrylic resin in cylindrical molds. The dentin occlusal surface was ground with 320-grit silicon carbide abrasive paper. The DBAs were prepared according to manufacturers' directions and applied on the dentin surface. Cylindrical teflon tubes were placed on the dentin surface and filled with a microfilled resin. The samples were then stored in a humidifier at 37 degrees C for 24 h. Six specimens were prepared for each group. A statistically significant difference was observed among the four groups. It has been observed that certain materials showed a dentin bond value superior to cohesive value of composite resin.
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PMID:[Dentinal bonding systems and the tensile bond strength test]. 194 60

In a previous study we reported no significant differences among the shear bond strengths resulting from the application of an orthodontic bonding resin to enamel surfaces etched with three phosphoric acid (H3PO4) concentrations, each for three etch durations. The objective of the current study was to determine the depths of etch on ground enamel surfaces exposed to the nine etching procedures. The facial surfaces of 45 extracted human maxillary permanent central incisors were ground wet on 600-grit silicon carbide paper. Annular adhesive disks of 6 mm outer diameter and 3 mm inner diameter were positioned on the ground enamel surfaces and etched with 10 mm3 of 37%, 15%, and 5% H3PO4 for 60, 30, and 15 seconds, respectively. The calcium concentrations of the etching solutions were determined and the depths of etch calculated. The depths of etch were then measured with a surface profilometer. A stepwise decrease in the calculated depths of etch with decreasing acid concentration and duration of etching was obtained. The calculated etch depths ranged from 27.1 microns by etching with 37% H3PO4 for 60 seconds to 3.5 microns by etching with 5% H3PO4 for 15 seconds. The measured depths of etch followed a similar pattern. A highly significant correlation between calculated and measured depths of etch was obtained.
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PMID:Effects of phosphoric acid concentration and etch duration on enamel depth of etch: an in vitro study. 219 1

To assess the effect of different rinse volumes and air and water pressures on shear enamel-composite resin bond strength, the buccal surfaces of 384 maxillary molars were prepared through 600-grit silicon carbide, gel-etched, and rinsed with one of 24 randomly assigned test conditions: 0, 2, 5, 10, 15, or 25 ml volume wash with air and water syringe pressures of 20/10, 20/40, 40/10, or 40/40 psi. The rinsed enamel was dried, Scotchbond adhesive was applied, and a polysiloxane ring was secured to the flattened surface. Silux resin was incrementally added to a depth of 2 mm and each increment cured 40 seconds. Shear bond strengths were determined by using an Instron testing machine at a crosshead speed of 0.5 mm/min. A statistically significant (p less than 0.05) volume effect was found only between the 0 volume rinse groups and each other volume group. No statistically significant differences (p less than 0.05) were seen between air or water pressure groups. Mean bond strengths for greater than or equal to 2 ml rinsing ranged from 250 +/- 30 to 280 +/- 50 kg/cm2. Enamel-composite resin bond strengths were not significantly increased beyond 2 ml rinsing regardless of air and water syringe pressure used.
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PMID:The effects of rinse volumes and air and water pressures on enamel-composite resin bond strength. 253 81

Enamel demineralization occurring adjacent to directly bonded orthodontic attachments is of great concern to orthodontists. The topical application of fluorides to enamel surfaces before acid etching and the bonding of the attachments is not recommended by many investigators. The objective of this study was to determine the enamel fluoride acquired from various topical fluoride agents and to determine the effect of the acquired fluoride on the tensile bond strength of an orthodontic bonding system. Fifty extracted maxillary central incisors were mounted in cups and the facial surfaces of the crowns were polished on 600-grit silicon carbide paper. Enamel microbiopsies were performed just off the midpoint of each tooth. Ten teeth served as controls and received no topical fluoride treatment, while a similar number were treated with either APF, SnF2, Duraphat, or Fluor Protector. The teeth were suspended in synthetic saliva 4 minutes after fluoride application. The topical fluoride agents were removed after 24 hours and the teeth were again suspended in synthetic saliva at 37 degrees C for 7 days. Enamel biopsies were again performed just off the midpoint of each tooth on the side not previously biopsied. The enamel surfaces were etched for 1 minute and the tensile bond strength of Concise orthodontic bonding system to the etched enamel surfaces was determined. The enamel surfaces acquired significantly different amounts of fluoride from the topical fluoride agents, but the bond strengths to these surfaces were not significantly different. The results of this in vitro study suggest that the application of topical fluoride agents to enamel surfaces 7 days before the bonding of orthodontic attachments will not have an adverse effect on bond strength.
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PMID:The effect of topical fluoride treatment on enamel fluoride uptake and the tensile bond strength of an orthodontic bonding resin. 315 23

The surface characteristics of eight posterior and two anterior composite resins were studied by SEM and profilometric tracings. The materials included both chemically cured and light-cured resin systems. Two posterior materials were microfilled composites; the others were conventional or hybrid types. The anterior composites were of conventional and hybrid types. At various steps in the procedures the following polishing/brushing treatments were evaluated: 1) dry polishing with Sof-lex discs followed by brushing with toothpaste; and 2) wet polishing with diamond pastes of increasing fineness, followed by brushing with toothpaste. The base line before the polishing/brushing procedures was obtained by wet polishing on silicon-carbide paper (4000 grit). All materials could be polished to a comparable smoothness by the Sof-lex discs, but this polishing procedure was associated with the development of an amorphous surface layer. Polishing with diamond pastes gave various results, with a 20-fold difference in surface roughness values from the smoothest to the roughest material. Toothbrushing after polishing with the Sof-lex system increased the surface roughness for all materials, but to various degrees. The two microfilled and four of the conventional posterior composites showed comparable surface roughness values, whereas two remaining posterior and the two anterior materials showed two to three times higher surface roughness values after toothbrushing.
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PMID:Surface characteristics of posterior composites after polishing and toothbrushing. 347 39


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